phosphate buffer in ethanol
cells of Acinetobacter calcoaceticus NCIMB 9871 presence; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Gagnon, Rene; Grogan, Gideon; Groussain, Esther; Pedragosa-Moreau, Sandrine; Richardson, Paul F.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 20 p. 2527 - 2528
1.1: acetic acid; zinc / 0 - 70 °C
2.1: C39H60N4O4; scandium tris(trifluoromethanesulfonate) / ethyl acetate / 0.5 h / 35 °C
2.2: 18 h / -40 °C
View Scheme
参考文献
Zhou, Lin; Liu, Xiaohua; Ji, Jie; Zhang, Yuheng; Hu, Xiaolei; Lin, Lili; Feng, Xiaoming
Journal of the American Chemical Society, 2012 , vol. 134, # 41 p. 17023 - 17026,4
1.1: trichlorophosphate / diethyl ether / |Reflux
2.1: acetic acid; zinc / 0 - 70 °C
3.1: C39H60N4O4; scandium tris(trifluoromethanesulfonate) / ethyl acetate / 0.5 h / 35 °C
3.2: 18 h / -40 °C
View Scheme
参考文献
Zhou, Lin; Liu, Xiaohua; Ji, Jie; Zhang, Yuheng; Hu, Xiaolei; Lin, Lili; Feng, Xiaoming
Journal of the American Chemical Society, 2012 , vol. 134, # 41 p. 17023 - 17026,4
