反应条件
1: 1.) n-BuLi / 1.) THF, hexane, -30 deg C, 30 min, 2.) THF, hexane, -30 deg C, 1 h
2: 1.) LDA / 1.) THF, -78 deg C, 1 h, 2.) THF, -78 deg C (1 h), -> 40 deg C
3: 1.) LiBH4, 2.) aq. HCl / 1.) THF, room temperature, 4 h, 2.) 1 h
4: 84 percent / PCC / CH2Cl2 / Ambient temperature
View Scheme
参考文献
Vanderlei, Jose Mauricio De L.; Coelho, Fernando; Almeida, Wanda P.
Synthetic Communications, 1998 , vol. 28, # 16 p. 3047 - 3055
