4-溴-5-硝基-异喹啉-1-甲醛合成路线 （共 5 条）
反应条件
selenium(IV) oxide in 1,4-dioxane 3 h; Heating;
参考文献
Liu, Mao-Chin; Lin, Tai-Shun; Penketh, Philip; Sartorelli, Alan C.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 21 p. 4234 - 4243
反应条件
1: 93 percent / 30percent aq. H2O2, glacial AcOH / 30 h / 65 - 70 °C 2: 60 percent / pyridine, Ac2O / CH2Cl2 / 36 h / 0 - 20 °C 3: 90 percent / 35percent aq. H2SO4 / 48 h / Heating 4: 91 percent / KNO3, H2SO4 / 2 h / 60 °C 5: 55 percent / SeO2 / dioxane / 3 h / Heating View Scheme
参考文献
Liu, Mao-Chin; Lin, Tai-Shun; Penketh, Philip; Sartorelli, Alan C.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 21 p. 4234 - 4243
反应条件
1: 60 percent / pyridine, Ac2O / CH2Cl2 / 36 h / 0 - 20 °C 2: 90 percent / 35percent aq. H2SO4 / 48 h / Heating 3: 91 percent / KNO3, H2SO4 / 2 h / 60 °C 4: 55 percent / SeO2 / dioxane / 3 h / Heating View Scheme
参考文献
Liu, Mao-Chin; Lin, Tai-Shun; Penketh, Philip; Sartorelli, Alan C.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 21 p. 4234 - 4243
反应条件
1: 91 percent / KNO3, H2SO4 / 2 h / 60 °C 2: 55 percent / SeO2 / dioxane / 3 h / Heating View Scheme
参考文献
Liu, Mao-Chin; Lin, Tai-Shun; Penketh, Philip; Sartorelli, Alan C.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 21 p. 4234 - 4243
反应条件
1: 90 percent / 35percent aq. H2SO4 / 48 h / Heating 2: 91 percent / KNO3, H2SO4 / 2 h / 60 °C 3: 55 percent / SeO2 / dioxane / 3 h / Heating View Scheme
参考文献
Liu, Mao-Chin; Lin, Tai-Shun; Penketh, Philip; Sartorelli, Alan C.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 21 p. 4234 - 4243
