2-甲基-4-苯基-3-丁炔-2-醇合成路线 （共 97 条）
反应条件
toluene-4-sulfonic acid in dichloromethane
4 h; Heating;
参考文献
Ishino; Mihara; Hayakawa; Miyata; Kaneko
Synthetic Communications, 2001 , vol. 31, # 3 p. 439 - 448
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium tert-butylate; silica gel in dimethyl sulfoxide
T=20 - 110°C; 0.05 h; Inert atmosphereMicrowave irradiation;
参考文献
Wu, Liansheng; Shi, Xiaokang; Xu, Xiaoyun; Liang, Fen; Huang, Guosheng
Journal of Chemical Sciences, 2011 , vol. 123, # 5 p. 697 - 702
反应条件
{(Pd{Fe(.eta.5-C5H5)(.eta.5-C5H3C(CH3)=NC6H4CH3-4)}(.mu.-Cl))2}; potassium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in acetonitrile
T=110°C; 16 h; Inert atmosphere;
参考文献
Hu, Hao; Yang, Fan; Wu, Yangjie
Journal of Organic Chemistry, 2013 , vol. 78, # 20 p. 10506 - 10511
反应条件
{(Pd{Fe(.eta.5-C5H5)(.eta.5-C5H3C(CH3)=NC6H4CH3-4)}(.mu.-Cl))2}; potassium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in acetonitrile
T=110°C; 16 h; Inert atmosphere;
参考文献
Hu, Hao; Yang, Fan; Wu, Yangjie
Journal of Organic Chemistry, 2013 , vol. 78, # 20 p. 10506 - 10511
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium tert-butylate; silica gel in dimethyl sulfoxide
T=20 - 110°C; 0.05 h; Inert atmosphereMicrowave irradiation;
参考文献
Wu, Liansheng; Shi, Xiaokang; Xu, Xiaoyun; Liang, Fen; Huang, Guosheng
Journal of Chemical Sciences, 2011 , vol. 123, # 5 p. 697 - 702
反应条件
in 1,2-dichloro-ethane
1 h; Molecular sieveReflux;
参考文献
Asakura, Noriaki; Hirokane, Tsukasa; Hoshida, Hayato; Yamada, Hidetoshi
Tetrahedron Letters, 2011 , vol. 52, # 4 p. 534 - 537
反应条件
iodine in dichloromethane
T=-20 - 25°C;
参考文献
Zhou, Chao; Chen, Xiaopeng; Lu, Ping; Wang, Yanguang
Tetrahedron, 2012 , vol. 68, # 13 p. 2844 - 2850
反应条件
[Cp*Ir(SnCl3)2{SnCl2(H2O)2}] in 1,2-dichloro-ethane
T=80°C; Inert atmosphereSchlenk technique; regioselective reaction;
参考文献
Maity, Arnab Kumar; Chatterjee, Paresh Nath; Roy, Sujit
Tetrahedron, 2013 , vol. 69, # 2 p. 942 - 956
反应条件
[Ir(COD)(SnCl3)Cl(μ-Cl)]2; 1,3-diphenyl-1,3-propanedione in 1,2-dichloro-ethane
T=80°C; 0.583333 h; Inert atmosphere;
参考文献
Chatterjee, Paresh Nath; Roy, Sujit
Tetrahedron, 2011 , vol. 67, # 25 p. 4569 - 4577
反应条件
[(η5-C5Me5)RuCl(μ2-SMe)2Ru(η5-C5Me5)(OH2)]OTf in 1,2-dichloro-ethane
T=60°C; 1 h;
参考文献
Nishibayashi, Yoshiaki; Inada, Youichi; Yoshikawa, Masato; Hidai, Masanobu; Uemura, Sakae
Angewandte Chemie - International Edition, 2003 , vol. 42, # 13 p. 1495 - 1498
