3,4,5-三甲氧基苯甲酸酐合成路线 （共 18 条）
反应条件
triethylamine; phenyl N-phenylphosphoroamidochloridate in dichloromethane 1 h; Ambient temperature;
参考文献
Mestres, Ramon; Palomo, Claudio
Synthesis, 1981 , # 3 p. 218 - 220
反应条件
N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate in toluene 0.75 h; Heating;
参考文献
Jaszay, Zsuzsa M.; Petnehazy, Imre; Toe, Laszlo
Heteroatom Chemistry, 2004 , vol. 15, # 6 p. 447 - 450
反应条件
in chloroform T=20°C; 24 h;
参考文献
Chechulina, L. A.; Puchkova, S. M.; Novikova, A. P.; Baskakova, Z. M.; Vysokov, V. I.; Afanas'eva, G. B.
Pharmaceutical Chemistry Journal, 1985 , vol. 19, # 3 p. 182 - 186
Khimiko-Farmatsevticheskii Zhurnal, 1985 , vol. 19, # 3 p. 168 - 172
反应条件
quinoline; chloroform
参考文献
Fischer,E.; Freudenberg
Chemische Berichte, 1913 , vol. 46, p. 1126,1128
参考文献
Sharp
Journal of the Chemical Society, 1936 , p. 1234
Full Text Show Details
Frank; Fanta; Tarbell
Journal of the American Chemical Society, 1948 , vol. 70, p. 2314,2317
反应条件
1: sodium-<3,4,5-trimethoxy benzoate> / 180 °C / Erwaermen des Reaktionsprodukts mit wss.-aethanol. Kalilauge 2: acetic acid anhydride; aqueous hydriodic acid View Scheme
参考文献
Charlesworth; Robinson
Journal of the Chemical Society, 1933 , p. 268
Full Text Show Details
Badhwar; Kang; Venkataraman
Journal of the Chemical Society, 1932 , p. 1107,1108
反应条件
1: sodium-<3,4,5-trimethoxy benzoate> / 180 °C / unter vermindertem Druck und Erwaermen des Reaktionsprodukts mit wss.-aethanol. Kalilauge 2: aq. NaOH solution View Scheme
参考文献
Rao et al.
Proceedings - Indian Academy of Sciences, Section A, 1944 , # 19 p. 88,91
反应条件
1: sodium-<3,4,5-trimethoxy benzoate> / 175 °C / anschliessend Erwaermen mit wss.-aethanol. Kalilauge und Erwaermen des Reaktionsprodukts mit Essigsaeure 2: pyridine 3: methanol; aqueous KOH-solution View Scheme
参考文献
Anderson
Canadian Journal of Research, 1932 , vol. 7, p. 285,289
参考文献
Ermakov, A. I.; Pleshkova, A. P.; Sorokin, A. A.; Skachilova, S. Ya.; Pleshakov, M. G.; Zuev, A. P.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 9 p. 1819 - 1825
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 9 p. 1986 - 1993
反应条件
1: With triethylamine Allan-Robinson condensation; 0.0833333 h; Heating; 2: With potassium hydroxide in methanol 0.333333 h; sonication;
参考文献
Daskiewicz, Jean-Baptiste; Depeint, Flore; Viornery, Lionel; Bayet, Christine; Comte-Sarrazin, Geraldine; Comte, Gilles; Gee, Jennifer M.; Johnson, Ian T.; Ndjoko, Karine; Hostettmann, Kurt; Barron, Denis
Journal of Medicinal Chemistry, 2005 , vol. 48, # 8 p. 2790 - 2804
