2-(3-甲氧羰基苯基)苯甲酸合成路线 （共 3 条）
反应条件
palladium(II) dichloride bis[bis(diphenylphosphine)ferrocene]; potassium carbonate in chloroform; water
T=80 - 100°C; Suzuki Coupling; 0.25 h;
参考文献
Bumagin; Veselov; Belov
Chemistry of Heterocyclic Compounds, 2014 , vol. 50, # 1 p. 19 - 25
Khim. Geterotsikl. Soedin., 2014 , vol. 50, # 1 p. 24 - 31,7
反应条件
trifluoroacetic acid in dichloromethane
T=20°C; 1 h;
参考文献
Li, Yan; Ding, Yan-Jun; Wang, Jian-Yong; Su, Yi-Ming; Wang, Xi-Sheng
Organic Letters, 2013 , vol. 15, # 11 p. 2574 - 2577
反应条件
1: potassium carbonate; tetra-(n-butyl)ammonium iodide / tetrahydrofuran / 6 h / |Reflux
2: sodium carbonate; Pd2(PPh3)2Cl2 / tetrahydrofuran; water / 60 °C / |Inert atmosphere
3: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
View Scheme
参考文献
Li, Yan; Ding, Yan-Jun; Wang, Jian-Yong; Su, Yi-Ming; Wang, Xi-Sheng
Organic Letters, 2013 , vol. 15, # 11 p. 2574 - 2577
