hydrogenchloride; hydrogen in methanol; water T=20°C; P=760.051 Torr; 32 h;

thionyl chloride T=-10 - 20°C; 16 h;

hydrogen; Nishimura catalyst <(45.9percent Rh/19.9percent Pt) oxide> in methanol T=25°C; P=75007.5 Torr;

hydrogenchloride in methanol T=20°C; 4 h;

chloro-trimethyl-silane Heating;

1: hydrogenchloride 2: 5 rhodium-on-charcoal; hydrogen / methanol; water / 16 h / 60 °C / 2828.7 - 3087.28 Torr 3: hydrogenchloride / methanol / 4 h / 20 °C View Scheme

1: 5 rhodium-on-charcoal; hydrogen / methanol; water / 16 h / 60 °C / 2828.7 - 3087.28 Torr 2: hydrogenchloride / methanol / 4 h / 20 °C View Scheme

1: 1,4-dioxane 2: triethylamine 3: lithium hydroxide hydrate; water / tetrahydrofuran View Scheme

1: 92 percent / NEt3 / CH2Cl2 / 1 h / 10 °C 2: 1.) sodium ethoxide, 2.) hydrochloric acid / 1.) ethanol, reflux, 5 min, 2.) water 3: 60 percent / ethanol; H2O / 25 h / Heating 4: hydrogen / platinum / methanol; ethyl acetate 5: 85 percent / p-toluenesulfonic acid / CH2Cl2; tetrahydrofuran / 24 h 6: 92 percent / 4-dimethylaminopyridine / tetrahydrofuran / 24 h View Scheme

hydrogenchloride 24 h; Reflux;