反应条件
1.1: potassium carbonate; potassium iodide / acetone; methanol / 25 - 35 °C / Inert atmosphere 1.2: pH 6 - 7 2.1: potassium tert-butylate / N,N-dimethyl-formamide / 0.5 h / -20 - -15 °C / Inert atmosphere 2.2: 1 h / -20 - -10 °C / pH 5 - 6 View Scheme
参考文献
GENERICS [UK] LIMITED; MYLAN INDIA PRIVATE LIMITED; GORE, Vinayak Govind; SHUKLA, Vinaykumar; MEKDE, Sandeep; HASBE, Suresh; BHANDARI, Sheryas; SHINDE, Dhananjay; PATIL, Madhukar Shaligram
Patent: WO2012/25762 A2, 2012 ;