反应条件
1: CH2Cl2 / 0.5 h / 0 °C
2: 1.) MeLi; 2.) tetrabutylammonium fluoride / 1.) THF, RT, 1 h; 2.) THF, 110 deg C, 10 h, sealed tube
View Scheme
参考文献
Tokitoh, Norihiro; Okazaki, Renji
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 9 p. 3291 - 3298
