1: Fmoc-L-phenylalanine With 4-methyl-morpholine; isobutyl chloroformate in tetrahydrofuran T=-15°C; 0.0833333 h; 2: diazomethane in tetrahydrofuran; diethyl ether T=-15 - 20°C; 0.5 h; Further stages.;
参考文献
Glenn, Matthew P.; Kelso, Michael J.; Tyndall, Joel D. A.; Fairlie, David P.
Journal of the American Chemical Society, 2003 , vol. 125, # 3 p. 640 - 641
Leggio, Antonella; Liguori, Angelo; Procopio, Antonio; Sindona, Giovanni
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 13 p. 1969 - 1971
potassium hydroxide in methanol; water T=20°C; 1.16667 h;
参考文献
Pinho, Vagner D.; Gutmann, Bernhard; Miranda, Leandro S. M.; De Souza, Rodrigo O. M. A.; Kappe, C. Oliver
Journal of Organic Chemistry, 2014 , vol. 79, # 4 p. 1555 - 1562
1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h / 20 °C 2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 20 °C 3: tetrahydrofuran / 2 h / 20 °C View Scheme
参考文献
Siciliano, Carlo; De Marco, Rosaria; Guidi, Ludovica Evelin; Spinella, Mariagiovanna; Liguori, Angelo
Journal of Organic Chemistry, 2012 , vol. 77, # 23 p. 10575 - 10582
1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h / 20 °C 2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 20 °C 3: tetrahydrofuran / 2 h / 20 °C View Scheme
参考文献
Siciliano, Carlo; De Marco, Rosaria; Guidi, Ludovica Evelin; Spinella, Mariagiovanna; Liguori, Angelo
Journal of Organic Chemistry, 2012 , vol. 77, # 23 p. 10575 - 10582
water; silver trifluoromethanesulfonate in 1,4-dioxane 72 h; sonication;
参考文献
Glenn, Matthew P.; Kelso, Michael J.; Tyndall, Joel D. A.; Fairlie, David P.
Journal of the American Chemical Society, 2003 , vol. 125, # 3 p. 640 - 641
