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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1721-92-2
合成路线
（共 45 条）
→
反应条件
1721-92-2
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tris-(dibenzylideneacetone)dipalladium(0) in toluene T=70°C; Suzuki-Miyaura cross-coupling; 1 h; Inert atmosphere;
参考文献
Li, Wenjie; Gao, Joe J.; Zhang, Yongda; Tang, Wenjun; Lee, Heewon; Fandrick, Keith R.; Lu, Bruce; Senanayake, Chris H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 10 p. 1671 - 1675
368-47-8
苯基三氟硅烷
+
4295-06-1
4-氯喹哪啶
→
反应条件
1721-92-2
反应条件
1: phenyl-trifluoro-silane With tetrabutyl ammonium fluoride; palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tert-butyl alcohol T=20°C; Hiyama cross-coupling reaction; 0.0833333 h; Inert atmosphereSealed vial; 2: 4-chloro-2-methyl-quinoline in tert-butyl alcohol T=60°C; Hiyama cross-coupling reaction; Inert atmosphereSealed vial;
参考文献
Molander, Gary A.; Iannazzo, Laura
Journal of Organic Chemistry, 2011 , vol. 76, # 21 p. 9182 - 9187
67-64-1
丙酮
+
5176-14-7
→
反应条件
1721-92-2
反应条件
1: 3-phenyl-2,1-benzisoxazole With samarium diiodide in tetrahydrofuran 0.0833333 h; Inert atmosphere; 2: acetone in tetrahydrofuran 1.5 h; Inert atmosphere;
参考文献
Stokes, Benjamin J.; Vogel, Carl V.; Urnezis, Linda K.; Pan, Minjie; Driver, Tom G.
Organic Letters, 2010 , vol. 12, # 12 p. 2884 - 2887
58109-40-3
二苯基碘六氟磷酸盐
+
536-74-3
苯乙炔
+
75-05-8
乙腈
→
反应条件
1721-92-2
反应条件
copper(II) bis(trifluoromethanesulfonate) in 1,2-dichloro-ethane T=120°C; Inert atmosphereSealed tube; regioselective reaction;
参考文献
Wang, Yong; Chen, Chao; Peng, Jing; Li, Ming
Angewandte Chemie - International Edition, 2013 , vol. 52, # 20 p. 5323 - 5327
Angew. Chem., 2013 , vol. 125, # 20 p. 5431 - 5435,5
611-35-8
4-氯喹啉
→
反应条件
1721-92-2
反应条件
1.1: tetrahydrofuran; hexane / 4 h / -78 °C 1.2: 90 percent / ammonium cerium(IV) nitrate / acetone; H2O / 0.5 h 2.1: 89 percent / dicyclohexylmethylamine; CsF / [(t-Bu)2P(OH)]2PdCl2 / dimethylformamide / 24 h / 135 °C View Scheme
参考文献
Wolf, Christian; Lerebours, Rachel
Journal of Organic Chemistry, 2003 , vol. 68, # 18 p. 7077 - 7084
5234-26-4
N-(2-乙酰苯基)乙酰胺
→
反应条件
1721-92-2
反应条件
1: tetrahydrofuran 2: 90 percent / polyphosphoric acid / 20 h / 160 °C View Scheme
参考文献
Curran, Dennis P.; Kuo, Shen-Chun
Journal of Organic Chemistry, 1984 , vol. 49, # 11 p. 2063 - 2065
607-67-0
4-羟基-2-甲基喹啉
→
反应条件
1721-92-2
反应条件
1: 4-methyl-morpholine / dichloromethane / 10 - 25 °C 2: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tris-(dibenzylideneacetone)dipalladium(0) / toluene / 2 h / 70 °C / Inert atmosphere View Scheme
参考文献
Li, Wenjie; Gao, Joe J.; Zhang, Yongda; Tang, Wenjun; Lee, Heewon; Fandrick, Keith R.; Lu, Bruce; Senanayake, Chris H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 10 p. 1671 - 1675
1318249-09-0
+
98-80-6
苯硼酸
→
反应条件
1721-92-2
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tris-(dibenzylideneacetone)dipalladium(0) in toluene T=70°C; Suzuki-Miyaura cross-coupling; 1 h; Inert atmosphere;
参考文献
Li, Wenjie; Gao, Joe J.; Zhang, Yongda; Tang, Wenjun; Lee, Heewon; Fandrick, Keith R.; Lu, Bruce; Senanayake, Chris H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 10 p. 1671 - 1675
1318249-10-3
+
98-80-6
苯硼酸
→
反应条件
1721-92-2
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tris-(dibenzylideneacetone)dipalladium(0) in toluene T=70°C; Suzuki-Miyaura cross-coupling; 1 h; Inert atmosphere;
参考文献
Li, Wenjie; Gao, Joe J.; Zhang, Yongda; Tang, Wenjun; Lee, Heewon; Fandrick, Keith R.; Lu, Bruce; Senanayake, Chris H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 10 p. 1671 - 1675
1318249-12-5
+
98-80-6
苯硼酸
→
反应条件
1721-92-2
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tris-(dibenzylideneacetone)dipalladium(0) in toluene T=70°C; Suzuki-Miyaura cross-coupling; 3 h; Inert atmosphere;
参考文献
Li, Wenjie; Gao, Joe J.; Zhang, Yongda; Tang, Wenjun; Lee, Heewon; Fandrick, Keith R.; Lu, Bruce; Senanayake, Chris H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 10 p. 1671 - 1675
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