3,5-二甲氧基苯甲酰氯合成路线 （共 90 条）
反应条件
thionyl chloride in N,N-dimethyl-formamide 18 h; Heating;
参考文献
Dol, Georg C.; Kamer, Paul C. J.; Van Leeuwen, Piet W. N. M.
European Journal of Organic Chemistry, 1998 , # 2 p. 359 - 364
参考文献
Japan Energy Corporation
Patent: US6310070 B1, 2001 ;
反应条件
1: 78 percent / hydrazine hydrate / 2 h / Heating 2: 63 percent / sodium nitrite, hydrochloric acid (2M), acetic acid (glacial) / H2O / 1 h / -10 °C 3: 93 percent / toluene / 2.5 h / Heating 4: 8.7 g / sodium hydroxide (20percent) / 60 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1658 - 1666
反应条件
1: 93 percent / toluene / 2.5 h / Heating 2: 8.7 g / sodium hydroxide (20percent) / 60 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1658 - 1666
反应条件
1: 63 percent / sodium nitrite, hydrochloric acid (2M), acetic acid (glacial) / H2O / 1 h / -10 °C 2: 93 percent / toluene / 2.5 h / Heating 3: 8.7 g / sodium hydroxide (20percent) / 60 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1658 - 1666
反应条件
1: NaOH 2: SOCl2 View Scheme
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 47, # 3 p. 167 - 174
反应条件
1: 8.7 g / sodium hydroxide (20percent) / 60 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1658 - 1666
反应条件
1: palladium/BaSO4; quinoline; sulfur / Hydrogenation.Reagens 4: Xylol 2: acetic acid anhydride; sodium acetate View Scheme
参考文献
Lambooy
Journal of the American Chemical Society, 1954 , vol. 76, p. 133,135
参考文献
Woodruff
Journal of the American Chemical Society, 1942 , vol. 64, p. 2859,2860
反应条件
diethyl ether und Erwaermen des Reaktionsprodukts mit Essigsaeure und wss.H2SO4;
参考文献
Abe et al.
Yakugaku Zasshi, 1956 , vol. 76, p. 1094
Chem.Abstr., 1957 , p. 2636
