3,5-二甲氧基苯甲酰胺合成路线 （共 34 条）
反应条件
ammonia; palladium diacetate; di-(1-adamantyl)-n-butylphosphine in 1,4-dioxane T=100°C; P=1500.15 Torr; 16 h; Autoclave;
参考文献
Tetrahedron Letters, , vol. 54, # 24 p. 3040 - 3042
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 87, p. 415
反应条件
sodium perborate; water in methanol T=50°C;
参考文献
McKillop, Alexander; Kemp, Duncan
Tetrahedron, 1989 , vol. 45, # 11 p. 3299 - 3306
反应条件
1: 78 percent / hydrazine hydrate / 2 h / Heating 2: 63 percent / sodium nitrite, hydrochloric acid (2M), acetic acid (glacial) / H2O / 1 h / -10 °C 3: 93 percent / toluene / 2.5 h / Heating 4: 8.7 g / sodium hydroxide (20percent) / 60 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1658 - 1666
反应条件
1: 93 percent / toluene / 2.5 h / Heating 2: 8.7 g / sodium hydroxide (20percent) / 60 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1658 - 1666
反应条件
1: 63 percent / sodium nitrite, hydrochloric acid (2M), acetic acid (glacial) / H2O / 1 h / -10 °C 2: 93 percent / toluene / 2.5 h / Heating 3: 8.7 g / sodium hydroxide (20percent) / 60 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1658 - 1666
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1658 - 1666
参考文献
Monatshefte fuer Chemie, , vol. 57, p. 52,58
反应条件
1: 84 percent / sodium hydroxide / heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1658 - 1666
反应条件
1: 8.7 g / sodium hydroxide (20percent) / 60 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1658 - 1666
