2-氯-1,2,3,4-四氢萘-1-酮合成路线 (共 16 条)
反应条件
N-chloro-succinimide; thiourea in methanol T=23°C; 0.166667 h;
参考文献
Mei, Yujiang; Bentley, Paul A.; Du, Juan
Tetrahedron Letters, 2008 , vol. 49, # 23 p. 3802 - 3804
反应条件
di((1R,2S,5R)-2-(iPr)-5-Me-cyclohexyl) N-Cl-imidodicarbonate in tetrahydrofuran; dichloromethane T=-78°C; 0.166667 h;
参考文献
Hajra, Saumen; Bhowmick, Manishabrata; Maji, Biswajit; Sinha, Debarshi
Journal of Organic Chemistry, 2007 , vol. 72, # 13 p. 4872 - 4876
反应条件
N,N-dichloro-p-toluenesulphonamide in acetonitrile T=40°C; 1.5 h;
参考文献
Kim, Yong Hae; Lee, In Sang; Lim, Sang Chul
Chemistry Letters, 1990 , # 7 p. 1125 - 1128
反应条件
lead(IV) acetate; sodium chloride in methanol T=0°C; 2 h;
参考文献
Motohashi, Shigeyasu; Satomi, Masakichi; Fujimoto, Yasuo; Tatsuno, Takashi
Synthesis, 1982 , # 12 p. 1021 - 1023
反应条件
lead(IV) acetate; calcium chloride in methanol T=0°C; 0.25 h;
参考文献
Motohashi, Shigeyasu; Satomi, Masakichi; Fujimoto, Yasuo; Tatsuno, Takashi
Synthesis, 1982 , # 12 p. 1021 - 1023
反应条件
amberlyst-15 in ethyl acetate T=20°C; 0.416667 h;
参考文献
Meshram; Reddy; Sadashiv; Yadav
Tetrahedron Letters, 2005 , vol. 46, # 4 p. 623 - 626
反应条件
iodobenzene dichloride T=20°C; 0.5 h; Molecular sieve;
参考文献
Yu, Jun; Zhang, Chi
Synthesis, 2009 , # 14 art. no. F02709SS, p. 2324 - 2328
反应条件
in cyclohexane 15 h; Irradiation; Product distributionMechanism;
参考文献
Sket, Boris; Zupan, Marko
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 8 p. 1745 - 1752
参考文献
Woroshzow; Koptjug
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 1646,1654; engl. Ausg. S. 1697, 1702, 1704
反应条件
1: 14 percent / tetrahydrofuran / 3 h / 0 °C 2: 35 percent Spectr. / ethylmagnesium bromide / benzene / 1) 0 deg C, 15 min; 2) reflux, 10 min View Scheme
参考文献
Gilchrist, Thomas L.; Stanford, John E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 225 - 230