triethylamine byproducts: H2; TEA was added in 9 portions at -196°C, after each addition stirring 2 h 0°C, 2 h at room temperature; then 4 days at room temperature; fractionated through traps, elem. anal.;
参考文献
Hosmane, Narayan S.; Sirmokadam, Narayan N.; Mollenhauser, Mark N.
Journal of Organometallic Chemistry, 1985 , vol. 279, p. 359 - 372
triethylamine byproducts: H2; TEA was added in 9 portions at -196°C, after each addition stirring 2 h 0°C, 2 h at room temperature; then 4 days at room temperature; fractionated through traps;
参考文献
Hosmane, Narayan S.; Sirmokadam, Narayan N.; Mollenhauser, Mark N.
Journal of Organometallic Chemistry, 1985 , vol. 279, p. 359 - 372
