hydrogenchloride; iron in ethanol Reduction; 3.5 h; Heating;
参考文献
Gudmundsson, Kristjan S.; Tidwell, Jeffrey; Lippa, Nicole; Koszalka, George W.; van Draanen, Nanine; Ptak, Roger G.; Drach, John C.; Townsend, Leroy B.
Journal of Medicinal Chemistry, 2000 , vol. 43, # 12 p. 2464 - 2472
1: With sodium dithionite; acetic acid in N,N-dimethyl-formamide
T=100°C; 15 h;
2: With sodium hydrogencarbonate in water; ethyl acetate; N,N-dimethyl-formamide