2-氯-6-硝基苯甲酸乙酯合成路线 （共 5 条）
反应条件
1: thionyl chloride View Scheme
参考文献
Goldstein; Preitner
Helvetica Chimica Acta, 1944 , vol. 27, p. 612,613
参考文献
Goldstein; Preitner
Helvetica Chimica Acta, 1944 , vol. 27, p. 612,613
反应条件
1: 95 percent / 25percent aq. TiCl3, AcOH / 0.15 h / Ambient temperature 2: 1.) aq. NaNO2, H2SO4 / 2.) 120 deg C, 1 h 3: 81 percent / K2CO3 / acetone / 3.5 h / Heating 4: 98 percent / 10percent aq. KOH / 3 h / Heating View Scheme
参考文献
Murakami; Watanabe; Otsuka; Iwata; Yamada; Yokoyama
Chemical and Pharmaceutical Bulletin, 1995 , vol. 43, # 8 p. 1287 - 1293
反应条件
1: 95 percent / 25percent aq. TiCl3, AcOH / 0.15 h / Ambient temperature 2: 1.) aq. NaNO2, H2SO4 / 2.) 120 deg C, 1 h View Scheme
参考文献
Murakami; Watanabe; Otsuka; Iwata; Yamada; Yokoyama
Chemical and Pharmaceutical Bulletin, 1995 , vol. 43, # 8 p. 1287 - 1293
反应条件
titanium(III) chloride; acetic acid 0.15 h; Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 43, # 8 p. 1287 - 1293
