3-(1-甲基乙氧基)-1,2-丙烷二醇合成路线 （共 9 条）
反应条件
palladium 10 on activated carbon; hydrogen
T=200°C; P=51755.2 Torr; 4 h;
参考文献
Dow Global Technologies LLC; TULCHINSKY, Michael, L.; BRIGGS, John, R.; RAND, Cynthia, L.
Patent: EP2318346 B1, 2013 ;
Location in patent: Paragraph 0088 ;
反应条件
tin(IV)tetraphenylporphyrinato trifluoromethanesulfonate; water in acetonitrile
2 h; Heating;
参考文献
Moghadam, Majid; Tangestaninejad, Shahram; Mirkhani, Valiollah; Shaibani, Reza
Tetrahedron, 2004 , vol. 60, # 29 p. 6105 - 6111
反应条件
hydrogen; palladium 10 on activated carbon
T=200°C; P=51716.2 Torr; 4 h; Inert atmosphere;
参考文献
Tulchinsky, Michael L.; Briggs, John R.; Rand, Cynthia L.
Patent: US2010/48940 A1, 2010 ;
Location in patent: Page/Page column 9-10 ;
反应条件
hydrogen; palladium 10 on activated carbon
T=200°C; P=51716.2 Torr; 4 h; Inert atmosphere;
参考文献
Tulchinsky, Michael L.; Briggs, John R.; Rand, Cynthia L.
Patent: US2010/48940 A1, 2010 ;
Location in patent: Page/Page column 10 ;
反应条件
palladium 10 on activated carbon; hydrogen
T=200°C; P=51755.2 Torr; 4 h;
参考文献
Dow Global Technologies LLC; TULCHINSKY, Michael, L.; BRIGGS, John, R.; RAND, Cynthia, L.
Patent: EP2318346 B1, 2013 ;
Location in patent: Paragraph 0089 ;
反应条件
1,1,3,3-tetramethyldisiloxane; palladium on carbon; camphor-10-sulfonic acid
T=60°C; 24 h; Inert atmosphere;
参考文献
Shi, Yan; Dayoub, Wissam; Chen, Guo-Rong; Lemaire, Marc
Tetrahedron Letters, 2011 , vol. 52, # 12 p. 1281 - 1283
反应条件
triethylsilane; boron trifluoride diethyl etherate in dichloromethane
T=20°C; 2 h;
参考文献
Cruz-Gregorio, Silvano; Sanchez, Mario; Clara-Sosa, Angel; Bernes, Sylvain; Quintero, Leticia; Sartillo-Piscil, Fernando
Journal of Organic Chemistry, 2005 , vol. 70, # 18 p. 7107 - 7113
反应条件
MCM-41-pr-TMEDA(+)Cl(-)
T=120°C; 4 h;
参考文献
Li, Jian; Wang, Liguo; Liu, Shimin; Li, Xueli; Shi, Feng; Deng, Youquan
Chemistry Letters, 2010 , vol. 39, # 12 p. 1277 - 1278
参考文献
Malinowskii; Wwedenskii
Zhurnal Obshchei Khimii, 1953 , vol. 23, p. 219; engl. Ausg. S. 227
