反应条件
1: 78 percent / p-TsOH / 70 h / Ambient temperature
2: 1) lithium aluminum hydride; 2) water, 15 percent NaOH / 1) ether, RT; 2) ether, 15 min
3: 93 percent / KH / tetrahydrofuran; hexane / 1 h
4: 80 percent / conc. HCl, water / methanol; H2O / Ambient temperature
5: 91 percent / Jones reagent / acetone / 0.13 h
View Scheme
参考文献
Nakata, Tadashi; Tani, Yoichiro; Hatozaki, Masayoshi; Oishi, Takeshi
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 4 p. 1411 - 1415