(9ci)-n-甲基-1H-苯并咪唑-2-胺合成路线 (共 7 条)
反应条件
in ethanol T=140°C; 12 h;
参考文献
Ueda, Satoshi; Buchwald, Stephen L.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 41 p. 10364 - 10367
反应条件
copper(l) iodide; caesium carbonate; N-methyl-2-(methylamino)ethylamine in N,N-dimethyl acetamide T=165°C; 16 h; Inert atmosphere;
参考文献
Deng, Xiaohu; McAllister, Heather; Mani, Neelakandha S.
Journal of Organic Chemistry, 2009 , vol. 74, # 15 p. 5742 - 5745
反应条件
sodium tetrahydroborate in ethanol 0.583333 h; Heating;
参考文献
Kemal, Oeznur; Reese, Colin B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1569 - 1573
反应条件
1: 87 percent / ethanol; H2O / 7 h / Heating 2: 76 percent / sodium borohydride / ethanol / 0.58 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1569 - 1573
反应条件
in nitrobenzene 5 h; Heating;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 24, # 9 p. 1012 - 1017
Khimiya Geterotsiklicheskikh Soedinenii, , # 9 p. 1226 - 1231
反应条件
in nitrobenzene 8 h; Heating;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 24, # 9 p. 1012 - 1017
Khimiya Geterotsiklicheskikh Soedinenii, , # 9 p. 1226 - 1231
反应条件
1: 88 percent / propan-1-ol / Heating 2: 25 percent / nitrobenzene / 8 h / Heating View Scheme
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 24, # 9 p. 1012 - 1017
Khimiya Geterotsiklicheskikh Soedinenii, , # 9 p. 1226 - 1231