反应条件
1: 1.) NaH, 2.) NaI / 1.) DMF, THF, light petroleum, reflux, 30 min, 2.) reflux, 24 h
2: 92 percent / LiAlH4 / diethyl ether / 4 h / Heating
3: tetrahydrofuran; CCl4 / -40 deg C -> 20 deg C
4: 8.84 g / NaOMe / methanol / 1.) 20 deg C, 16 h, 2.) reflux, 4 h
View Scheme
参考文献
Kocienski, Philip; Todd, Michael
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1783 - 1789
