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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
172293-43-5
合成路线
（共 9 条）
591220-94-9
→
反应条件
172293-43-5
反应条件
trimethylsilyl bromide in acetonitrile T=40°C; 4 h;
参考文献
Rajwanshi, Vivek K.; Prhavc, Marija; Fagan, Patrick; Brooks, Jennifer L.; Hurd, Tiffany; Cook, P. Dan; Wang, Guangyi
Nucleosides, Nucleotides and Nucleic Acids, 2005 , vol. 24, # 3 p. 179 - 189
172293-42-4
→
反应条件
172293-43-5
反应条件
trimethylsilyl bromide in dichloromethane T=25°C; 7 h;
参考文献
Hakimelahi; Moosavi-Movahedi; Sadeghi; Tsay; Jih Ru Hwu
Journal of Medicinal Chemistry, 1995 , vol. 38, # 23 p. 4648 - 4659
172293-47-9
→
反应条件
172293-43-5
反应条件
trimethylsilyl bromide in dichloromethane T=25°C; 7 h;
参考文献
Hakimelahi; Moosavi-Movahedi; Sadeghi; Tsay; Jih Ru Hwu
Journal of Medicinal Chemistry, 1995 , vol. 38, # 23 p. 4648 - 4659
7481-90-5
1-(3,5-脱水-2-脱氧-Β-D-苏-戊呋喃糖基)胸腺嘧啶
→
反应条件
172293-43-5
反应条件
1: 70 percent / BF3*OEt2, LiBr / tetrahydrofuran / 2 h / -50 °C 2: 40 percent / 20 h / 140 °C 3: 98 percent / diethyl ether 4: 95 percent / pyridine, 4-(dimethylamino)pyridine / 24 h / 20 °C 5: 69 percent / LiN3 / dimethylformamide / 4 h / 95 °C 6: 75 percent / Me3SiBr / CH2Cl2 / 7 h / 25 °C View Scheme
参考文献
Hakimelahi; Moosavi-Movahedi; Sadeghi; Tsay; Jih Ru Hwu
Journal of Medicinal Chemistry, 1995 , vol. 38, # 23 p. 4648 - 4659
499970-82-0
→
反应条件
172293-43-5
反应条件
1: 48 percent / 3 h / 180 °C 2: 64 percent / NaOEt / ethanol / 3 h / 0 °C 3: 92 percent / DMAP; pyridine / 13 h / 20 °C 4: 55 percent / NaN3 / dimethylformamide / 14 h / 60 °C 5: TMSBr / acetonitrile / 4 h / 40 °C View Scheme
参考文献
Rajwanshi, Vivek K.; Prhavc, Marija; Fagan, Patrick; Brooks, Jennifer L.; Hurd, Tiffany; Cook, P. Dan; Wang, Guangyi
Nucleosides, Nucleotides and Nucleic Acids, 2005 , vol. 24, # 3 p. 179 - 189
591220-93-8
→
反应条件
172293-43-5
反应条件
1: 92 percent / DMAP; pyridine / 13 h / 20 °C 2: 55 percent / NaN3 / dimethylformamide / 14 h / 60 °C 3: TMSBr / acetonitrile / 4 h / 40 °C View Scheme
参考文献
Rajwanshi, Vivek K.; Prhavc, Marija; Fagan, Patrick; Brooks, Jennifer L.; Hurd, Tiffany; Cook, P. Dan; Wang, Guangyi
Nucleosides, Nucleotides and Nucleic Acids, 2005 , vol. 24, # 3 p. 179 - 189
591220-91-6
→
反应条件
172293-43-5
反应条件
1: 64 percent / NaOEt / ethanol / 3 h / 0 °C 2: 92 percent / DMAP; pyridine / 13 h / 20 °C 3: 55 percent / NaN3 / dimethylformamide / 14 h / 60 °C 4: TMSBr / acetonitrile / 4 h / 40 °C View Scheme
参考文献
Rajwanshi, Vivek K.; Prhavc, Marija; Fagan, Patrick; Brooks, Jennifer L.; Hurd, Tiffany; Cook, P. Dan; Wang, Guangyi
Nucleosides, Nucleotides and Nucleic Acids, 2005 , vol. 24, # 3 p. 179 - 189
591220-92-7
→
反应条件
172293-43-5
反应条件
1: 55 percent / NaN3 / dimethylformamide / 14 h / 60 °C 2: TMSBr / acetonitrile / 4 h / 40 °C View Scheme
参考文献
Rajwanshi, Vivek K.; Prhavc, Marija; Fagan, Patrick; Brooks, Jennifer L.; Hurd, Tiffany; Cook, P. Dan; Wang, Guangyi
Nucleosides, Nucleotides and Nucleic Acids, 2005 , vol. 24, # 3 p. 179 - 189
94892-66-7
→
反应条件
172293-43-5
反应条件
1: 77 percent / pyridine / 17 h / 20 °C 2: 48 percent / 3 h / 180 °C 3: 64 percent / NaOEt / ethanol / 3 h / 0 °C 4: 92 percent / DMAP; pyridine / 13 h / 20 °C 5: 55 percent / NaN3 / dimethylformamide / 14 h / 60 °C 6: TMSBr / acetonitrile / 4 h / 40 °C View Scheme
参考文献
Rajwanshi, Vivek K.; Prhavc, Marija; Fagan, Patrick; Brooks, Jennifer L.; Hurd, Tiffany; Cook, P. Dan; Wang, Guangyi
Nucleosides, Nucleotides and Nucleic Acids, 2005 , vol. 24, # 3 p. 179 - 189
