4,4’-(1,2-乙亚基)双吗啉合成路线 （共 15 条）
反应条件
[Ru(tris(2,2'-bipyridyl))3]Cl2·6H2O; water; oxygen; silica gel; caesium carbonate in acetonitrile T=20°C; 60 h; Inert atmosphereIrradiation;
参考文献
Zhao, Yaohong; Cai, Shunyou; Li, Jing; Wang, David Zhigang
Tetrahedron, 2013 , vol. 69, # 38 p. 8129 - 8131
反应条件
sodium tetrahydroborate in tetrahydrofuran
T=20°C;
参考文献
Katritzky, Alan R.; Fan, Wei-Qiang; Fu, Cong
Journal of Organic Chemistry, 1990 , vol. 55, # 10 p. 3209 - 3213
反应条件
N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide in water
T=70 - 80°C;
参考文献
Markosyan; Baghdasaryan; Oganesyan; Attaryan; Asratyan
Russian Journal of General Chemistry, 2012 , vol. 82, # 2 p. 344 - 345
反应条件
6 h; RefluxInert atmosphere;
参考文献
Zhao, Yaohong; Cai, Shunyou; Li, Jing; Wang, David Zhigang
Tetrahedron, 2013 , vol. 69, # 38 p. 8129 - 8131
反应条件
N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide in water
T=70 - 80°C; 2.5 h;
参考文献
Markosyan; Baghdasaryan; Oganesyan; Attaryan; Asratyan
Russian Journal of General Chemistry, 2012 , vol. 82, # 2 p. 344 - 345
参考文献
Hultquist; Northey
Journal of the American Chemical Society, 1940 , vol. 62, p. 447
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Geigy A.G.
Patent: CH206717 , 1938 ;
反应条件
iron(II) chloride in chloroform
T=-78°C; 5 h;
参考文献
Rosenau; Potthast; Sixta; Kosma
Tetrahedron, 2002 , vol. 58, # 15 p. 3073 - 3078
反应条件
1: With iron(II) chloride in chloroform
T=-78°C; 0.5 h;
2: With sulfuric acid in chloroform
T=-78°C;
参考文献
Rosenau; Potthast; Sixta; Kosma
Tetrahedron, 2002 , vol. 58, # 15 p. 3073 - 3078
参考文献
Anderson et al.
Journal of the Chemical Society, 1956 , p. 4088,4090
Full Text Show Details
Mason; Malkiel
Journal of the American Chemical Society, 1940 , vol. 62, p. 1448
反应条件
sulfuric acid
T=160 - 170°C; im Rohr;
参考文献
Knorr; Brownsdon
Chemische Berichte, 1902 , vol. 35, p. 4474
