3-((苄氧基)甲基)环丁酮合成路线 （共 21 条）
反应条件
L-Selectridereg; in tetrahydrofuran T=-78°C; Yield given. Yields of byproduct given;
参考文献
PFIZER LIMITED
Patent: WO2006/92691 A1, 2006 ;
Location in patent: Page/Page column 78 ;
反应条件
1: 84 percent / L-Selectride / tetrahydrofuran / -78 °C 2: 50 percent / Ph3P; DEAD / tetrahydrofuran / 20 °C 3: 88 percent / NaOH / dioxane / 20 °C View Scheme
参考文献
Kaiwar, Vijay; Reese, Colin B.; Gray, Emily J.; Neidle, Stephen
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 18 p. 2281 - 2288
反应条件
phosphate buffer in ethanol T=27°C; the fungus Cunninghamella echinulata NRRL 3655, in fermentor 450 rpm, 30 L/h air;
参考文献
Mazzini; Lebreton; Alphand; Furstoss
Journal of Organic Chemistry, 1997 , vol. 62, # 15 p. 5215 - 5218
反应条件
phosphate buffer in ethanol NADPH-dependent monooxygenase from Pseudomonas putida NCIMB 10007 presence; Title compound not separated from byproducts;
参考文献
Rudroff, Florian; Rydz, Joanna; Ogink, Freek H.; Fink, Michael; Mihovilovic, Marko D.
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 8-9 p. 1436 - 1444
反应条件
1: 95 percent / PTSA / benzene 2: H2 / Pd/C / methanol View Scheme
参考文献
Kabalka, George W.; Yao, Min-Liang
Tetrahedron Letters, 2003 , vol. 44, # 9 p. 1879 - 1881
反应条件
hydrogen; palladium 10 on activated carbon in methanol; water T=20°C; P=760.051 Torr; 1 h;
参考文献
US2011/86882 A1, ;
Page/Page column 24 ;
US 20110086882 A1
反应条件
hydrogen bromide
7 h; Heating;
参考文献
Rammeloo, Thomas; Stevens, Christian V.; De Kimpe, Norbert
Journal of Organic Chemistry, 2002 , vol. 67, # 18 p. 6509 - 6513
反应条件
toluene-4-sulfonic acid in benzene
参考文献
Kabalka, George W.; Yao, Min-Liang
Tetrahedron Letters, 2003 , vol. 44, # 9 p. 1879 - 1881
反应条件
toluene-4-sulfonic acid in benzene
参考文献
Kabalka, George W.; Yao, Min-Liang
Journal of Organic Chemistry, 2004 , vol. 69, # 24 p. 8280 - 8286
反应条件
1: 95 percent / PTSA / benzene
2: H2 / Pd/C / methanol
View Scheme
参考文献
Kabalka, George W.; Yao, Min-Liang
Tetrahedron Letters, 2003 , vol. 44, # 9 p. 1879 - 1881
