反应条件
in diethyl ether; toluene
addn. of trichlorostanne in toluene to soln. of arylmagnesium bromide in ether (cooling), removal of ether (distn. off), heating (90°C, 3 h); addn. of aq. HCl, sepn. and drying of org. layer (CaCl2), removal of solvent (evapn., vac.), crystn. (MeOH); elem. anal.;
参考文献
Pombrik, S. I.; Peregudov, A. S.; Fedin, E. I.; Kravtsov, D. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, p. 2092 - 2096
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , vol. 31, p. 2375 - 2379
