O,O’-双(三甲基硅烷)-5-氟尿嘧啶合成路线 （共 39 条）
反应条件
in dichloromethane; water
参考文献
Yamasa Shoyu Kabushiki Kaisha
Patent: US5334593 A1, 1994 ;
反应条件
O-(2,4,6-trimethylbenzenesulfonyl)hydroxylamine in dichloromethane
4 h; Ambient temperature;
参考文献
Imaizumi; Kano; Sakata
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 7 p. 1808 - 1813
参考文献
Zhuk, R. A.; Ludzisha, A. S.; Kostyanovskii, R. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 1 p. 74 - 77
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 1 p. 90 - 93
反应条件
in acetonitrile
4 h; Heating;
参考文献
Zhang, Zhouen; Hatta, Hiroshi; Ito, Takeo; Nishimoto, Sei-Ichi
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 4 p. 592 - 596
反应条件
in acetonitrile
1) room temp., 2 h; 2) reflux, 2 h; 3) room temp., overnight.;
参考文献
Schwarz; Cech; Holy; Skoda
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 11 p. 3217 - 3230
参考文献
Karpeiskii, M. Ya.; Mikhailov, S. M.; Tsieminya, A. S.; Ziderman, A. A.; Kravchenko, I. M.; et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , vol. 16, # 11 p. 1176 - 1179
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , vol. 16, # 11 p. 1541 - 1544
反应条件
pyridine in 1,4-dioxane
5 h; Ambient temperature;
参考文献
Yamashita; Yamawaki; Ueda; Yasumoto; Unemi; Hashimoto
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 12 p. 4258 - 4267
参考文献
Karpeiskii, M. Ya.; Mikhailov, S. M.; Tsieminya, A. S.; Ziderman, A. A.; Kravchenko, I. M.; et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , vol. 16, # 11 p. 1176 - 1179
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , vol. 16, # 11 p. 1541 - 1544
反应条件
N-bromosuccinmide; 4 A molecular sieve in dichloromethane
T=-78°C; Yields of byproduct given;
参考文献
Sujino, Keiko; Yoshida, Tomoyasu; Sugimura, Hideyuki
Tetrahedron Letters, 1996 , vol. 37, # 34 p. 6133 - 6136
