3-N-Boc-3-N-甲胺基哌啶合成路线 （共 6 条）
反应条件
hydrogen; 5 rhodium-on-charcoal in ethanol T=25°C; P=3102.97 Torr; 27 h; Paar apparatus;
参考文献
US2005/159423 A1, ;
Page/Page column 18 ;
反应条件
1: With sodium hydride in DMF (N,N-dimethyl-formamide) T=20°C; 4 h; 2: With hydrogen; palladium on activated charcoal in ethanol T=20°C; 5 h;
参考文献
EP1568699 A1, ;
Page/Page column 42 ;
反应条件
hydrogen; palladium on activated charcoal in ethanol Ambient temperature;
参考文献
Barlocco, Daniela; Villa, Stefania; Fratta, Walter; Fadda, Paola; Colombo, Diego; Toma, Lucio
Tetrahedron, 1995 , vol. 51, # 42 p. 11547 - 11556
反应条件
1: 71 percent / NaBH4 / methanol; H2O / 1 h / Ambient temperature 2: 85 percent / CH2Cl2 3: 90 percent / H2 / 10percent Pd/C / ethanol / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 51, # 42 p. 11547 - 11556
反应条件
1: 85 percent / CH2Cl2 2: 90 percent / H2 / 10percent Pd/C / ethanol / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 51, # 42 p. 11547 - 11556
反应条件
1: 80 percent / 1 h / 100 °C 2: 87 percent / HCl / diethyl ether / Ambient temperature View Scheme
参考文献
Barlocco, Daniela; Villa, Stefania; Fratta, Walter; Fadda, Paola; Colombo, Diego; Toma, Lucio
Tetrahedron, 1995 , vol. 51, # 42 p. 11547 - 11556
