4-(1-丙炔-1-基)苯甲醛合成路线 （共 5 条）
反应条件
copper(l) iodide; tris(dibenzylideneacetone)dipalladium (0); triphenylphosphine; triethylamine T=80°C; Sonogashira cross-coupling reaction; 24 h;
参考文献
Zhang, Wei; Kraft, Stefan; Moore, Jeffrey S.
Journal of the American Chemical Society, 2004 , vol. 126, # 1 p. 329 - 335
反应条件
B-OMe-9-borabicyclo[3.3.1]nonane; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran Heating;
参考文献
Fuerstner, Alois; Seidel, Guenter
Tetrahedron, 1995 , vol. 51, # 41 p. 11165 - 11176
反应条件
tris[N-(tert-butyl)(3,5-dimethylphenyl)amido]molybdenum(VI) propylidyne; tris(2-hydroxy-5-nitro-benzyl)amine in tetrachloromethane T=40°C; 7 h; Inert atmosphere;
参考文献
Jyothish, Kuthanapillil; Zhang, Wei
Angewandte Chemie - International Edition, 2011 , vol. 50, # 15 p. 3435 - 3438
反应条件
C34H44MoO3Si in tetrachloromethane
T=40°C; 16 h; Inert atmosphereMolecular sieve; Reagent/catalystSolvent;
参考文献
The Regents of the University of Colorado, a body corporate; Zhang, Wei; Kuthanapillil, Jyothish; Wang, Qi
Patent: US2013/261295 A1, 2013 ;
Location in patent: Paragraph 0281; 0282 ;
反应条件
tris[N-(tert-butyl)(3,5-dimethylphenyl)amido]molybdenum(VI) propylidyne; tris(2-hydroxy-5-nitro-benzyl)amine in tetrachloromethane
T=40°C; 7 h; Inert atmosphere;
参考文献
Jyothish, Kuthanapillil; Zhang, Wei
Angewandte Chemie - International Edition, 2011 , vol. 50, # 15 p. 3435 - 3438
