11-叠氮基-3,6,9-三氧代十一酸合成路线 （共 18 条）
反应条件
1: 95 percent / NaN3 / dimethylformamide / 3 h / 60 °C 2: 96 percent / KOH / H2O; tetrahydrofuran / 6 h / 20 °C View Scheme
参考文献
Newkome, George R.; Kotta, Kishore K.; Mishra, Amaresh; Moorefield, Charles N.
Macromolecules, 2004 , vol. 37, # 22 p. 8262 - 8268
反应条件
1: Et3N / diethyl ether 2: NaN3 / ethanol / Heating 3: 80 percent / CrO3; aq. H2SO4 / acetone View Scheme
参考文献
Leal, Manuel Pernia; Assali, Mohyeddin; Fernandez, Inmaculada; Khiar, Noureddine
Chemistry - A European Journal, 2011 , vol. 17, # 6 p. 1828 - 1836
反应条件
1: NaN3 / ethanol / Heating 2: 80 percent / CrO3; aq. H2SO4 / acetone View Scheme
参考文献
Leal, Manuel Pernia; Assali, Mohyeddin; Fernandez, Inmaculada; Khiar, Noureddine
Chemistry - A European Journal, 2011 , vol. 17, # 6 p. 1828 - 1836
反应条件
1: 5.42 g / sodium azide / aq. ethanol / Heating 2: 76 percent / KOH / dimethylformamide / 24 h / 45 °C View Scheme
参考文献
Sang Won Jeong; O'Brien
Journal of Organic Chemistry, 2001 , vol. 66, # 14 p. 4799 - 4802
反应条件
1: 96 percent / NaN3 / dimethylformamide / 5 h / 100 °C 2: 90 percent / LiOH / methanol; H2O / Ambient temperature View Scheme
参考文献
Boumrah, Deradji; Campbell, Malcolm M.; Fenner, Simon; Kinsman, Richard G.
Tetrahedron Letters, 1991 , vol. 32, # 52 p. 7735 - 7738
反应条件
1.1: sodium azide / N,N-dimethyl-formamide / 16 h / 20 °C 2.1: potassium tert-butylate / tert-butyl alcohol / 0.25 h / 30 °C 2.2: 16 h / 30 °C 3.1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C View Scheme
参考文献
Devigny, Christian; Perez-Balderas, Francisco; Hoogeland, Bastiaan; Cuboni, Serena; Wachtel, Rudolf; Mauch, Christoph P.; Webb, Katharine J.; Deussing, Jan M.; Hausch, Felix
Journal of the American Chemical Society, 2011 , vol. 133, # 23 p. 8927 - 8933
反应条件
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / |Inert atmosphere 2: chromium(VI) oxide; sulfuric acid / acetone; water / 0 - 20 °C View Scheme
参考文献
Liao, Longyan; Liu, Jenny; Dreaden, Erik C.; Morton, Stephen W.; Shopsowitz, Kevin E.; Hammond, Paula T.; Johnson, Jeremiah A.
Journal of the American Chemical Society, 2014 , vol. 136, # 16 p. 5896 - 5899
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Boumrah, Derradji; Campbell, Malcolm M.; Fenner, Simon; Kinsman, Richard G.
Tetrahedron, 1997 , vol. 53, # 20 p. 6977 - 6992
