反应条件
1.1: diethyl ether / -78 - 20 °C
2.1: dihydrogen peroxide; sulfuric acid / tetrahydrofuran; water / 8 h / 0 - 60 °C
3.1: copper diacetate; 1,10-phenanthroline; triethylamine; oxygen / toluene; acetonitrile / 20 °C
3.2: 20 °C
4.1: diethyl ether; hexane / -78 - 20 °C
5.1: chloro-trimethyl-silane / dichloromethane / 2 h / 20 °C
6.1: palladium 10 on activated carbon; hydrogen / ethanol / 2 h / 20 °C
View Scheme
参考文献
Too, Pei Chui; Tnay, Ya Lin; Chiba, Shunsuke
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1217 - 1225
