(1-苯基-1-丁烯)苯合成路线 (共 59 条)
反应条件
2: tBuMgBr
View Scheme
参考文献
Eisch,J.J.; Merkley,J.H.
Journal of the American Chemical Society, 1979 , vol. 101, # 5 p. 1148 - 1155
参考文献
Hill et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 1663
反应条件
rhodium-carbene-complex in toluene
T=50°C; 6 h;
参考文献
Wolf, Justin; Brandt, Lutz; Fries, Arno; Werner, Helmut
Angewandte Chemie, 1990 , vol. 102, # 5 p. 584 - 586
反应条件
in diethyl ether; hexane
3 h; Ambient temperature;
参考文献
Araki, Shuki; Jin, Shun-Ji; Butsugan, Yasuo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 5 p. 549 - 552
反应条件
1: 89 percent / DMAP, Py / 16 h / Ambient temperature
2: 78 percent / NaH, DBU / tetrahydrofuran / 3.5 h / Ambient temperature
3: 2.) H2O / 1.) THF, 0 deg C, 30 min.
View Scheme
参考文献
Satoh, Tsuyoshi; Takano, Koji; Hiroyuki, Ota; Someya, Hideaki; Matsuda, Kenji; Koyama, Mai
Tetrahedron, 1998 , vol. 54, # 21 p. 5557 - 5574
反应条件
1: 78 percent / NaH, DBU / tetrahydrofuran / 3.5 h / Ambient temperature
2: 2.) H2O / 1.) THF, 0 deg C, 30 min.
View Scheme
参考文献
Satoh, Tsuyoshi; Takano, Koji; Hiroyuki, Ota; Someya, Hideaki; Matsuda, Kenji; Koyama, Mai
Tetrahedron, 1998 , vol. 54, # 21 p. 5557 - 5574
反应条件
cyclohexa-1,4-diene; Triethylzinnwasserstoff in cyclohexane
T=110°C; Decomposition; Product distribution; Further Variations:ReagentsTemperaturesSolvents;
参考文献
Halgren, Thomas A.; Roberts, John D.; Horner, John H.; Martinez, Felix N.; Tronche, Christopher; Newcomb, Martin
Journal of the American Chemical Society, 2000 , vol. 122, # 13 p. 2988 - 2994
反应条件
cyclohexa-1,4-diene in cyclohexane
T=35°C; Decomposition; Product distribution; Further Variations:initial concrntrations;
参考文献
Halgren, Thomas A.; Roberts, John D.; Horner, John H.; Martinez, Felix N.; Tronche, Christopher; Newcomb, Martin
Journal of the American Chemical Society, 2000 , vol. 122, # 13 p. 2988 - 2994
反应条件
in diethyl ether
3 h; Ambient temperature;
参考文献
Ohno, Atsuyoshi; Uohama, Misao; Oka, Shinzaburo
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 10 p. 3231 - 3232
参考文献
Klages; Heilmann
Chemische Berichte, 1904 , vol. 37, p. 1452