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hydroxylammonium sulfate; magnesium methanolate multistep reaction: 1.) MeOH, toluene, reflux, 1 h, 2.) 95 deg C, 1.25 h, 3.) H2O, 55 deg C, 1 h; magnesium-mediated ortho-specific formylation and formaldoximation of substituted phenols, effect of the substituent; Product distribution;

in diethyl ether 1.) -70 grad C, 2 h, 2.) 0 grad C, 4 h, 3.) room temperature, 3 days;

ammonium formate; palladium on activated charcoal in methanol T=20°C; 16 h;