alpha-甲基环己-3-烯-1-甲醇合成路线 （共 11 条）
反应条件
lithium borohydride; borane in tetrahydrofuran T=-50°C; 2 h;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 7 p. 855 - 856
反应条件
dichloro bis(acetonitrile) palladium(II); Ru2(CO)4(μ-H)(C4Ph4-COHOC-C4Ph4); water; p-benozquinone in methanol; isopropyl alcohol T=85°C; 48 h; Inert atmosphereGlovebox; regioselective reaction;
参考文献
Chemical Communications, , vol. 50, # 20 p. 2608 - 2611
反应条件
in 1,2-dichloro-ethane T=60°C; 2 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 57, # 2 p. 446 - 451
反应条件
(i) Et2O, (ii) aq. NH4Cl; Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 101, p. 6648 - 6656
反应条件
oxygen; tri-isobutyl aluminium; zirconocene dichloride 1.) (CH2Cl)2, 0 deg C, 24 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 21, p. 1501 - 1504
反应条件
magnesium; methyl iodide in diethyl ether 0.25 h; Heating;
参考文献
Farmaco, Edizione Scientifica, , vol. 35, # 6 p. 441 - 446
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 1, p. 2148 - 2156
Zhurnal Organicheskoi Khimii, , vol. 1, # 12 p. 2105 - 2115
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Wilcox,C.F.; Chibber,S.S.
Journal of Organic Chemistry, 1962 , vol. 27, p. 2332 - 2338
反应条件
tert.-butylhydroperoxide; benzyltrimethylammonium tetrabromooxomolybate(V) in benzene
T=60°C; 24 h;
参考文献
Masuyama, Yoshiro; Takahashi, Masato; Kurusu, Yasuhiko
Tetrahedron Letters, 1984 , vol. 25, # 39 p. 4417 - 4420
参考文献
Petrow; Sopow
Zhurnal Obshchei Khimii, 1952 , vol. 22, p. 591,595, 599; engl. Ausg. S. 653, 655, 659
