2-甲基-2-丙基[(2R)-1-氰基-3-甲基-2-丁烷基]氨基甲酸酯合成路线 (共 4 条)
反应条件
hydrogenchloride 12 h; Heating;
参考文献
Sott, Richard; Granander, Johan; Williamson, Carl; Hilmersson, Goeran
Chemistry - A European Journal, 2005 , vol. 11, # 16 p. 4785 - 4792
反应条件
1: 6 M HCl / 12 h / Heating 2: aq. NaOH / 1.) 0 deg C, 0.5 h, 2.) room temperature, 2 h View Scheme
参考文献
Sutherland, Andrew; Willis, Christine L.
Journal of Organic Chemistry, 1998 , vol. 63, # 22 p. 7764 - 7769
反应条件
hydrogenchloride 12 h; Heating;
参考文献
Sott, Richard; Granander, Johan; Williamson, Carl; Hilmersson, Goeran
Chemistry - A European Journal, 2005 , vol. 11, # 16 p. 4785 - 4792
反应条件
1: TFA / CH2Cl2 / 1 h 2: 10 percent aq. Na2CO3 / tetrahydrofuran / 1 h / Ambient temperature 3: 91 percent / conc. aq. HCl / dioxane / 8 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 51, # 45 p. 12337 - 12350