3,5-二乙氧基基苯甲酸甲酯合成路线 （共 48 条）
参考文献
Journal of the American Chemical Society, , vol. 70, p. 662
反应条件
1: 84 percent / sodium hydroxide / heating 2: 88 percent / conc. sulphuric acid / 16 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1658 - 1666
反应条件
1: 8.7 g / sodium hydroxide (20percent) / 60 °C 2: 88 percent / conc. sulphuric acid / 16 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1658 - 1666
参考文献
Chemische Berichte, , vol. 35, p. 2885 Anm.
反应条件
1: 78 percent / hydrazine hydrate / 2 h / Heating 2: 63 percent / sodium nitrite, hydrochloric acid (2M), acetic acid (glacial) / H2O / 1 h / -10 °C 3: 93 percent / toluene / 2.5 h / Heating 4: 8.7 g / sodium hydroxide (20percent) / 60 °C 8: 28.8 g / fluoroboric acid, sodium nitrite / H2O 9: 7.6 g / warming, distillation 10: 52 percent / lithium chips / 0.75 h 11: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C View Scheme
参考文献
Durrani, Aziz A.; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1658 - 1666
反应条件
1: 78 percent / hydrazine hydrate / 2 h / Heating 2: 63 percent / sodium nitrite, hydrochloric acid (2M), acetic acid (glacial) / H2O / 1 h / -10 °C 3: 93 percent / toluene / 2.5 h / Heating 4: 8.7 g / sodium hydroxide (20percent) / 60 °C 8: 28.8 g / fluoroboric acid, sodium nitrite / H2O 9: 7.6 g / warming, distillation 10: 60 percent / lithium chips / 0.5 h 11: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C View Scheme
参考文献
Durrani, Aziz A.; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1658 - 1666
反应条件
1: (i) Mg, Et2O, (ii) /BRN= 2105670/ 2: Py / CH2Cl2 View Scheme
参考文献
Birr,C. et al.
Justus Liebigs Annalen der Chemie, 1972 , vol. 763, p. 162 - 172
反应条件
(i) Mg, Et2O, (ii) /BRN= 2105670/; Multistep reaction;
参考文献
Birr,C. et al.
Justus Liebigs Annalen der Chemie, 1972 , vol. 763, p. 162 - 172
反应条件
hydrazine hydrate 2 h; Heating;
参考文献
Durrani, Aziz A.; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1658 - 1666
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 20 °C / |Inert atmosphere 2: hydrogenchloride / water / |Inert atmosphere 3: 10 h / 140 °C / |Inert atmosphere 4: potassium hydroxide / tetrahydrofuran / 24 h / |Inert atmosphere 5: methyl iodide; magnesium / diethyl ether / 45 - 190 °C / |Inert atmosphere 6: triethylamine / dichloromethane / 4 h / |Inert atmosphere View Scheme
参考文献
Jungong, Christian S.; Novikov, Alexei V.
Synthetic Communications, 2012 , vol. 42, # 24 p. 3589 - 3597,9
Title/Abstract Full Text Show Details
Jungong, Christian S.; Novikov, Alexei V.
Synthetic Communications, 2012 , vol. 42, # 24 p. 3589 - 3597
