1-苯基十八烷-1,3-二酮合成路线 （共 6 条）
反应条件
sodium methylate in anhydrous xylene Claisen Condensation; 1.25 h; Inert atmosphereRefluxMicrowave irradiation;
参考文献
DEXERA; Honnart, Stephane; Galy-Jammou, Philippe
Patent: US2014/88325 A1, 2014 ;
Location in patent: Paragraph 0139; 0140; 0141; 0142; 0143 ;
反应条件
in tetrahydrofuran; water; dimethyl sulfoxide
参考文献
Ciba-Geigy Corporation
Patent: US5344992 A1, 1994 ;
反应条件
1: magnesium; ethanol; tetrachloromethane / diethyl ether 2: NaCl; DMSO / H2O / 8 h / Heating View Scheme
参考文献
Schulz, Stefan; Arsene, Cristian; Tauber, Marianne; McNeil, Jeremy N.
Phytochemistry, 2000 , vol. 54, # 3 p. 325 - 336
反应条件
1: magnesium; ethanol; tetrachloromethane / diethyl ether 2: NaCl; DMSO / H2O / 8 h / Heating View Scheme
参考文献
Schulz, Stefan; Arsene, Cristian; Tauber, Marianne; McNeil, Jeremy N.
Phytochemistry, 2000 , vol. 54, # 3 p. 325 - 336
反应条件
sodium; xylene T=130°C;
参考文献
Wiemann et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1954 , vol. 238, p. 699
参考文献
Wiemann et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1954 , vol. 238, p. 699
