1-(2-乙氧基-2-氧乙基)溴化吡啶合成路线 （共 15 条）
参考文献
KANG, Dong-Min; CHAE, Mi-Young; KANG, Myeong-Soon; JUNG, Sung-Hyun; JUNG, Ho-Kuk; LEE, Nam-Heon; KIM, Nam-Soo
Patent: US2012/313091 A1, 2012 ;
Location in patent: Page/Page column 69-70 ;
反应条件
in acetonitrile T=20°C; Knoevenagel condensation; 2 h;
参考文献
Journal of Combinatorial Chemistry, , vol. 12, # 2 p. 260 - 265
反应条件
in acetonitrile T=20°C; Knoevenagel condensation; 2 h;
参考文献
Journal of Combinatorial Chemistry, , vol. 12, # 2 p. 260 - 265
反应条件
in acetonitrile T=20°C; Knoevenagel condensation; 2 h;
参考文献
Journal of Combinatorial Chemistry, , vol. 12, # 2 p. 260 - 265
参考文献
Lukes; Pliml
Collection of Czechoslovak Chemical Communications, 1956 , vol. 21, p. 1602,1605
反应条件
1: 93 percent / Triethylamine / ethanol / 20 h / Heating 2: 10percent NaOH / methanol / 3 h / Heating 3: PPA / 1 h / 100 °C 4: 58 percent / Raney-Nickel (W-2) / ethanol / 20 h / Heating View Scheme
参考文献
Tominaga, Yoshinori; Shiroshita, Yoshihide; Kurokawa, Tomohiko; Gotou, Hiromi; Matsuda, Yoshiro; Hosomi, Akira
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 477 - 487
参考文献
Lukes; Pliml
Collection of Czechoslovak Chemical Communications, 1956 , vol. 21, p. 1602,1605
反应条件
triethylamine in ethanol Heating;
参考文献
Tominaga, Yoshinori; Ichihara, Yuichi; Mori, Tomoko; Kamio, Chizuko; Hosomi, Akira
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 2 p. 263 - 268
反应条件
1: benzoyl chloride; phenylacetylene With copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=20°C; Sonogashira coupling reaction; 2 h; 2: 1-[(ethoxycarbonyl)methyl]pyridinium bromide in tetrahydrofuran T=20°C; 14 h;
参考文献
Helvetica Chimica Acta, , vol. 88, # 7 p. 1798 - 1812
反应条件
potassium carbonate in tetrahydrofuran Ambient temperature;
参考文献
Journal of Heterocyclic Chemistry, , vol. 28, # 1 p. 45 - 48
