acetic acid in water 4 h; Heating;

1: 83 percent / potassium t-butoxide / tetrahydrofuran / 3 h / -15 °C 2: 81 percent / hydrogen / 10 percent palladium on charcoal / ethanol / 5 h / 2327.17 Torr / Ambient temperature 3: 32 percent / 33 percent acetic acid / H2O / 4 h / Heating View Scheme

1: 81 percent / hydrogen / 10 percent palladium on charcoal / ethanol / 5 h / 2327.17 Torr / Ambient temperature 2: 32 percent / 33 percent acetic acid / H2O / 4 h / Heating View Scheme

1: 2.) H2 / 2.) Pd/C / 1.) reflux, 3 h, 2.) toluene 2: 1.) phosphorus oxychloride, 2.) conc. HCl / 1.) 0 deg C, 1 h, 2.) MeOH, THF, RT, 45 min View Scheme

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hydrogenchloride; trichlorophosphate 1.) 0 deg C, 1 h, 2.) MeOH, THF, RT, 45 min; Yield given. Multistep reaction;

hydrogen bromide in acetic acid T=100°C; 2 h;