1-甲基咪唑-5-甲酸甲酯合成路线 （共 18 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=-10 - 36°C; 3 h;
参考文献
Kirchlechner; Casutt; Heywang; Schwarz
Synthesis, 1994 , # 3 p. 247 - 248
反应条件
1: 80 percent / lithium aluminum hydride / tetrahydrofuran / 3 h / -10 - 36 °C 2: MnO2 / tetrahydrofuran / Heating View Scheme
参考文献
Jones; McLaughlin
Journal of the American Chemical Society, 1949 , vol. 71, p. 2444,2447
反应条件
sulfuric acid; dimethyl sulfate in methanol; water; acetic anhydride
参考文献
BASF Aktiengesellschaft
Patent: US4864030 A1, 1989 ;
反应条件
sodium hydroxide T=80°C; 18 h;
参考文献
Schering Corporation
Patent: US2004/122018 A1, 2004 ;
Location in patent: Page 349 ;
参考文献
Jones; McLaughlin
Journal of the American Chemical Society, 1949 , vol. 71, p. 2444,2447
反应条件
1: LiAlH4; diethyl ether 2: SOCl2 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 71, p. 2444,2447
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane T=60°C; 50 h;
参考文献
O'Connell, John F.; Parquette, Jonathan; Yelle, William E.; Wang, Wilhelm; Rapoport, Henry
Synthesis, 1988 , # 10 p. 767 - 771
反应条件
trichloromonobromomethane; N-bromoacetamide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane T=50°C; 60 h;
参考文献
O'Connell, John F.; Parquette, Jonathan; Yelle, William E.; Wang, Wilhelm; Rapoport, Henry
Synthesis, 1988 , # 10 p. 767 - 771
