2-(N-甲基-n-苯基氨基甲基)苯硼酸合成路线 (共 2 条)
反应条件
1: With acetic anhydride in acetonitrile T=0°C; 3 h; Molecular sieve; 2: With sodium tris(acetoxy)borohydride in acetonitrile T=0°C; 0.166667 h; Molecular sieve; Further stages;
参考文献
Adamczyk-Wozniak, Agnieszka; Fratila, Raluca M.; Madura, Izabela D.; Pawelko, Alicja; Sporzynski, Andrzej; Tumanowicz, Marta; Velders, Aldrik H.; Yla, Jacek
Tetrahedron Letters, 2011 , vol. 52, # 49 p. 6639 - 6642
反应条件
n-butyllithium; H2O in tetrahydrofuran org. compound was lithiated at -78°, B(OMe)3 added at -78°C, hydrolyzed at room temp.; elem. anal.;
参考文献
Sandanayake, K. R. A. Samankumara; Shinkai, Seiji
Journal of the Chemical Society, Chemical Communications, 1994 , # 9 p. 1083 - 1084