4-甲氧基-6-苯基-5,6-二氢-2H-吡喃-2-酮合成路线 （共 16 条）
反应条件
1: With lithium diisopropyl amide 2: With oxonium
参考文献
Lokot'; Pashkovskii; Lakhvich
Chemistry of Heterocyclic Compounds, 2001 , vol. 37, # 6 p. 707 - 714
反应条件
n-butyllithium; trimethylphosphane in hexane; dichloromethane
T=22°C; 0.5 h;
参考文献
Creech, Gardner S.; Kwon, Ohyun
Organic Letters, 2008 , vol. 10, # 3 p. 429 - 432
反应条件
1: anhydrous zinc chloride / CH2Cl2 / 1.) -78 deg C; 2.) r.t., overnight
2: H2O / Ambient temperature
View Scheme
参考文献
Midland, M. Mark; Graham, Richard S.
Journal of the American Chemical Society, 1984 , vol. 106, # 15 p. 4294 - 4296
反应条件
1: anhydrous zinc chloride / CH2Cl2 / 1.) -78 deg C; 2.) r.t., overnight
2: H2O / Ambient temperature
View Scheme
参考文献
Midland, M. Mark; Graham, Richard S.
Journal of the American Chemical Society, 1984 , vol. 106, # 15 p. 4294 - 4296
反应条件
potassium carbonate in acetone
4 h; Heating;
参考文献
Lokot'; Pashkovskii; Lakhvich
Chemistry of Heterocyclic Compounds, 2001 , vol. 37, # 6 p. 707 - 714
反应条件
palladium (II) trifluoroacetate; (+/-)-3,5,3',5'-tBu4Phbox; p-benozquinone
T=20°C;
参考文献
Motodate, Satoshi; Kobayashi, Takuya; Fujii, Mikio; Mochida, Tomoyuki; Kusakabe, Taichi; Katoh, Shigeki; Akita, Hiroyuki; Kato, Keisuke
Chemistry - An Asian Journal, 2010 , vol. 5, # 10 p. 2221 - 2230
反应条件
zinc in 1,4-dioxane
3 h; Heating;
参考文献
Abramson; Wormser
Journal of Heterocyclic Chemistry, 1981 , vol. 18, # 2 p. 363 - 366
参考文献
Henbest; Jones
Journal of the Chemical Society, 1950 , p. 3628,3631
Full Text Show Details
Reid; Ruby
Journal of the American Chemical Society, 1951 , vol. 73, p. 1054,1058
参考文献
Henbest; Jones
Journal of the Chemical Society, 1950 , p. 3628,3631
Full Text Show Details
Reid; Ruby
Journal of the American Chemical Society, 1951 , vol. 73, p. 1054,1058
反应条件
(4R,5R)-1-benzyl-4-((3-(4,5-bis(hydroxydinaphthalen-1-ylmethyl)-1,3-dioxolan-2-yl)phenoxy)methyl)-3-methyl-1H-1,2,3-triazol-3-ium tetrafluoroborate in methanol
T=24°C; Diels-Alder Cycloaddition; P=7.50075 Torr; 48 h; Catalytic behavior; Reagent/catalystSolventTemperature;
参考文献
Yacob, Zekarias; Liebscher, Juergen
Arkivoc, 2012 , vol. 2012, # 3 p. 312 - 319
