(2R,5R)-2,5-己二醇合成路线 （共 27 条）
反应条件
lithium hydroxide in methanol T=25°C; 8 h;
参考文献
Kim, Mahn-Joo; Lee, In Suk; Jeong, Nakcheol; Choi, Yoon Kyung
Journal of Organic Chemistry, 1993 , vol. 58, # 23 p. 6483 - 6485
反应条件
sodium methylate in methanol T=0°C; electrochemical coupling, pH 5.38;
参考文献
Burk; Feaster; Harlow
Tetrahedron Asymmetry, 1991 , vol. 2, # 7 p. 569 - 592
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0°C; 1 h;
参考文献
Li, Xiaoyong; Burrell, Carmin E.; Staples, Richard J.; Borhan, Babak
Journal of the American Chemical Society, 2012 , vol. 134, # 22 p. 9026 - 9029
反应条件
(Ph)2SiH2; potassium carbonate; bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate; (S,S)-2,2''-bis[(R)-1-(diethylphosphino)ethyl]-1,1'-biferrocene 1.) DME, -30 degC, 30 h; 2.) MeOH; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 36, # 29 p. 5239 - 5242
反应条件
potassium carbonate in methanol; water 12 h; Ambient temperature;
参考文献
Whitesell, James K.; Reynolds, Dan
Journal of Organic Chemistry, 1983 , vol. 48, # 20 p. 3548 - 3551
反应条件
lithium aluminium tetrahydride in tetrahydrofuran; diethyl ether 24 h; Ambient temperature;
参考文献
Saravana, P.; Raina, Sushil; Sambamurthy, T.; Singh, Vinod K.
Journal of Organic Chemistry, 1997 , vol. 62, # 8 p. 2669 - 2670
反应条件
yeast Pichia farinosa IAM 4682 in a glucose medium T=30°C; 48 h;
参考文献
Ikeda; Sato; Sugai; Ohta
Tetrahedron, 1996 , vol. 52, # 24 p. 8113 - 8122
参考文献
Solladie, Guy; Huser, Nathalie; Garcia-Ruano, Jose Luis; Adrio, Javier; Carmen Carreno; Tito, Amelia
Tetrahedron Letters, 1994 , vol. 35, # 29 p. 5297 - 5300
反应条件
Rhodococcus ruber DSM 44541 in acetone T=30°C; pH=7.5; 48 h;
参考文献
European Journal of Organic Chemistry, , # 8 p. 1904 - 1909
反应条件
2: 100 percent / LiOH*H2O / methanol / 8 h / 25 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 23 p. 6483 - 6485
