1,3,5-三(氯甲基)苯合成路线 （共 5 条）
反应条件
lithium chloride in N,N-dimethyl-formamide T=0 - 20°C; 2.5 h; Inert atmosphere;
参考文献
Hermes, Jens Peter; Sander, Fabian; Peterle, Torsten; Urbani, Raphael; Pfohl, Thomas; Thompson, Damien; Mayor, Marcel
Chemistry - A European Journal, 2011 , vol. 17, # 48 p. 13473 - 13481
反应条件
pyridine; thionyl chloride in benzene
参考文献
Cochrane,W.P. et al.
Journal of the Chemical Society [Section] C: Organic, 1968 , p. 630 - 632
反应条件
1: LiAlH4 / diethyl ether 2: SOCl2, Py / benzene View Scheme
参考文献
Cochrane,W.P. et al.
Journal of the Chemical Society [Section] C: Organic, 1968 , p. 630 - 632
反应条件
1: 80 percent / KCN, 18-crown-6 / acetonitrile / 144 h / Ambient temperature 2: 98 percent / conc. H2SO4, H2O / 5 h / Heating View Scheme
参考文献
Kanishi, Masayuki; Kunizaki, Jun-ichi; Inanaga, Junji; Yamaguchi, Masaru
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 12 p. 3828 - 3831
反应条件
lt;Mg(anthracene)(THF)3gt;
1.) THF, 20 deg C, 1 h, 2.) THF; Yield given. Multistep reaction;
参考文献
Harvey, Stephen; Junk, Peter C.; Raston, Colin L.; Salem, Geoffrey
Journal of Organic Chemistry, 1988 , vol. 53, # 14 p. 3134 - 3140
