Barber, Christopher; Bury, Paul; Kocienski, Philip; O'Shea, Michael
Journal of the Chemical Society, Chemical Communications, 1991 , # 22 p. 1595 - 1597
water; ammonium chloride in diethyl ether
to soln. of Bu3SnCHCl(OEt) in anhyd. Et2O added dropwise soln. of CH2CHCH2MgBr in anhyd. Et2O at 0 °C, after 1 h at 0 °C added satd. aq. soln. of NH4Cl; extd. (Et2O), org. layer dried (MgSO4), distd. in vac. or chromd. (SiO2, pentane);
参考文献
Quintard, Jean-Paul; Elissondo, Bernard; Hattich, Thomas; Pereyre, Michel
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 149 - 162
Didier, Charles; Critcher, Douglas J.; Walshe, Nigel D.; Kojima, Yasuhiro; Yamauchi, Yuji; Barrett, Anthony G. M.
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