UNIVERSITY OF PRINCE EDWARD ISLAND; GENESIS GROUP INC.; SHAVER, Michael, P.; KOZAK, Christopher, M.
Patent: WO2013/53046 A1, 2013 ;
Location in patent: Paragraph 00193-00195 ;
1: 2-propenylmagnesium bromide With manganese (II) chloride in tetrahydrofuran Metallation; 2: α,α,α',α'-tetrabromo-o-xylene in tetrahydrofuran T=0°C; Substitution; 2.5 h; 3: With water Substitution;
参考文献
Kakiya; Shinokubo; Oshima
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 9 p. 2139 - 2147