hydrogen; triethylamine; {RuHCl((R)-2,2'-bis(diphenylphosphino)-1,1'-binaphthyl)2} in tetrahydrofuran; ethanol T=50°C; P=2280 Torr; 24 h; Yield given. Title compound not separated from byproducts;
参考文献
Journal of Organometallic Chemistry, , vol. 428, # 1-2 p. 155 - 167
1: With (CuOTf)2.C6H6; (2-diphenylphosphinobenzoyl)-Thr(O-t-Bu)-D-Val-NH-n-butyl in toluene T=0°C; 1.3 h; 2: With lithium hydroxide; dihydrogen peroxide in tetrahydrofuran Title compound not separated from byproducts;
参考文献
Angewandte Chemie - International Edition, , vol. 42, # 11 p. 1276 - 1279