1-(2-溴苯基)-1-甲基乙胺合成路线 （共 5 条）
反应条件
in water; acetonitrile
参考文献
Oxis Isle of Man, Limited
Patent: US5968920 A1, 1999 ;
反应条件
bis-[(trifluoroacetoxy)iodo]benzene in water; acetonitrile T=20°C; 24 h;
参考文献
Erdelmeier; Tailhan-Lomont; Yadan
Journal of Organic Chemistry, 2000 , vol. 65, # 24 p. 8152 - 8157
反应条件
1: 90 percent / aq. K2CO3; conc. H2O2 / ethanol / 14 h / 20 °C 2: 83 percent / bis(trifluoroacetoxy)iodobenzene / acetonitrile; H2O / 24 h / 20 °C View Scheme
参考文献
Erdelmeier; Tailhan-Lomont; Yadan
Journal of Organic Chemistry, 2000 , vol. 65, # 24 p. 8152 - 8157
反应条件
2: 84 percent / sulfuric acid / acetic acid / 24 h / 20 - 45 °C 3: 97 percent / sodium hydroxide / H2O / 24 h / Heating View Scheme
参考文献
Toyota, Shinji; Asakura, Mitsuhiro; Futawaka, Tadahiro; Oki, Michinori
Bulletin of the Chemical Society of Japan, 1999 , vol. 72, # 8 p. 1879 - 1885
反应条件
1: 84 percent / sulfuric acid / acetic acid / 24 h / 20 - 45 °C 2: 97 percent / sodium hydroxide / H2O / 24 h / Heating View Scheme
参考文献
Toyota, Shinji; Asakura, Mitsuhiro; Futawaka, Tadahiro; Oki, Michinori
Bulletin of the Chemical Society of Japan, 1999 , vol. 72, # 8 p. 1879 - 1885
