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dihydrogen hexachloroplatinate in isopropyl alcohol T=80°C;

Hydrolysis.anschliessende Umsetzung mit Kaliumacetat;

lithium aluminium tetrahydride Reduction;

triethylamine in pentane

1: 68 percent / Irradiation 2: 63 percent / LiAlH4 / diethyl ether View Scheme

triethylamine in pentane T=20°C; 2 h;

n-BuLi in tetrahydrofuran; hexane byproducts: LiCl; (Ar); std. Schlenk technique; soln. of Fe complex in THF was treated with soln. of BuLi in hexane at -78°C for 90 min; warmed to -30°C; soln. of Si compd. in THF was added dropwise; warmed to room temp.; stirred for 14 h; concd.; treated with hexane; filtered; solvent removed; chromd. (silica gel, hexane); solvent removed; elem. anal.;