triethylamine; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in benzene 14 h; Heating;

triethylamine; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in benzene 14 h; Heating;

Ni(PCy3)2Cl2 in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=90°C; Negishi coupling reaction; 8 h; Inert atmosphere;

triethylamine; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in benzene 14 h; Heating;

triethylamine; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in benzene 14 h; Heating;

triethylamine; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in benzene 14 h; Heating;

C32H26ClN2NiOP in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=85°C; 12 h; Inert atmosphere;

methyl iodide in ammonia Irradiation (UV/VIS); condensation of sodium-dried ammonia into round-bottomed Pyrex flask, addn. of Me3SnCl and Na, addn. of CH3OC6H4NMe3I; irradn. with stirring for30 min, quenching by addn. of MeI in excess; evapn. of ammonia, treatment with water, extn. with ether;

C32H26ClN2NiP in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=85°C; 12 h; Inert atmosphere;