(3,3-二甲基丁基)苯合成路线 （共 33 条）
反应条件
cyclohexa-1,4-diene; potassium tert-butylate in dimethyl sulfoxide
T=20°C; 3 h; Schlenk techniqueInert atmosphereIrradiationGreen chemistry;
参考文献
Oksdath-Mansilla, Gabriela; Argueello, Juan E.; Penenory, Alicia B.
Tetrahedron Letters, 2013 , vol. 54, # 12 p. 1515 - 1518
反应条件
in diethyl ether
T=-78°C;
参考文献
Wei, Xudong; Johnson, Paul; Taylor, Richard J.K.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 7 p. 1109 - 1116
反应条件
sodium hydroxide; hydrazine hydrate in various solvent(s)
4 h; Heating;
参考文献
Kilway, Kathleen V.; Siegel, Jay S.
Journal of the American Chemical Society, 1992 , vol. 114, # 1 p. 255 - 261
反应条件
zirconocene dichloride; 1,1-dimethylethylmagnesium chloride in diethyl ether; benzene
Ambient temperature;
参考文献
Negishi, Ei-ichi; Miller, Joseph A.; Yoshida, Tadao
Tetrahedron Letters, 1984 , vol. 25, # 32 p. 3407 - 3410
反应条件
1: With tris-(dibenzylideneacetone)dipalladium(0); tri-cyclo-hexyl-phosphine in 1,4-dioxane
T=20°C; 0.25 h; Inert atmosphere;
2: With formic acid in 1,4-dioxane
T=80°C; Inert atmosphere; stereoselective reaction;
参考文献
Shen, Ruwei; Chen, Tieqiao; Zhao, Yalei; Qiu, Renhua; Zhou, Yongbo; Yin, Shuangfeng; Wang, Xiangbo; Goto, Midori; Han, Li-Biao
Journal of the American Chemical Society, 2011 , vol. 133, # 42 p. 17037 - 17044
反应条件
potassium hydroxide; hydrazine hydrate; diethylene glycol
T=190°C;
参考文献
Berliner; Berliner
Journal of the American Chemical Society, 1950 , vol. 72, p. 222,223
反应条件
1: 64 percent / AlCl3 / 18 h / Heating
2: 75 percent / 55percent aq. NH2NH2, NaOH / various solvent(s) / 4 h / Heating
View Scheme
参考文献
Kilway, Kathleen V.; Siegel, Jay S.
Journal of the American Chemical Society, 1992 , vol. 114, # 1 p. 255 - 261
反应条件
1: 64 percent / AlCl3 / 18 h / Heating
2: 75 percent / 55percent aq. NH2NH2, NaOH / various solvent(s) / 4 h / Heating
View Scheme
参考文献
Kilway, Kathleen V.; Siegel, Jay S.
Journal of the American Chemical Society, 1992 , vol. 114, # 1 p. 255 - 261
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate
参考文献
Eisch,J.J.; Amtmann,R.
Journal of Organic Chemistry, 1972 , vol. 37, p. 3410 - 3415
反应条件
in dichloromethane
T=-78°C; 0.5 h;
参考文献
Ooi, Takashi; Uraguchi, Daisuke; Kagoshima, Naoko; Maruoka, Keiji
Tetrahedron Letters, 1997 , vol. 38, # 32 p. 5679 - 5682
